HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14025391, compound → HCID 54434705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14025391 | HCID 14025391 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54434705 | HCID 54434705 | 97% |
Reaction Steps
In accordance with Example No. 3, 22.7 g of (5-chloro-3-methoxy-2-nitrophenyl)acetonitrile dissolved in a 100 ml/70 ml mixture of THF/37% HCl were reduced with 26 g of zinc powder. 19 g of (2-amino-5-chloro-3-methoxyphenyl)acetonitrile were obtained (yield=97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05876465 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-f27001886a504a48bfbdab24b4c12a20 |
| Source note | uspto-grants-1999_03 |