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HRID1417320

反应详情

EQUATION

反应方程式

HRID 1417320 的结构方程式

REACTANTS

反应物

2
结构：COC(OC)N(C)C
HCID78373

Methanamine, 1,1-dimethoxy-N,N-dimethyl-

C5H13NO2

结构：CC(=O)c1ccc(OCCCCN2C(=O)c3ccccc3C2=O)cc1
HCID67598087

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)/C=C/C(=O)c1ccc(OCCCCN2C(=O)c3ccccc3C2=O)cc1
HCID67693872

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

A solution of 25 g of 2-[4-(4-acetylphenoxy)butyl]-1H-isoindole-1,3(2H)-dione (Example 42) and 25 ml of dimethylformamide dimethylacetal in 50 ml of dioxane is heated in the steam bath for 16 hours. The volatile components are removed in vacuo, a tacky reddish-brown solid being obtained. A portion is recrystallized from dichloromethane/hexane; m.p. 109°-111° C.

WORKUP

后处理

  1. customThe volatile components are removed in vacuo
  2. customa tacky reddish-brown solid being obtained
  3. customA portion is recrystallized from dichloromethane/hexane