HRID1417353

反应详情

EQUATION

反应方程式

HRID 1417353 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

4-Aminobenzoic acid (17.24 g, 0.1257 mol) was added to a stirred solution of maleic anhydride (12.33 g, 0.1257 mol) in propanone (300 ml). Stirring was continued at room temperature for 3 hours. The product, which separated as a yellow solid, was collected by suction filtration and dried on the filter: mp 217°-219° C. (Ref: K C Liu, J. Chin. Chem. Soc., 1973, 20, 163).

WORKUP

后处理

  1. customThe product, which separated as a yellow solid
  2. filtrationwas collected by suction filtration
  3. customdried on the
  4. filtrationfilter