Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Aminobenzoic Acid → (Z)-4-(3-carboxyacrylamido)benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Aminobenzoic Acid | HCID 978 | — |
| 반응물 | Maleic Anhydride | HCID 7923 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | (Z)-4-(3-carboxyacrylamido)benzoic acid | HCID 5717537 | — |
반응 단계
4-Aminobenzoic acid (17.24 g, 0.1257 mol) was added to a stirred solution of maleic anhydride (12.33 g, 0.1257 mol) in propanone (300 ml). Stirring was continued at room temperature for 3 hours. The product, which separated as a yellow solid, was collected by suction filtration and dried on the filter: mp 217°-219° C. (Ref: K C Liu, J. Chin. Chem. Soc., 1973, 20, 163).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05877204 |
| 출처 데이터셋 | uspto-grants-1999_03 |
| ORD ID | ord-6a5a3a0446f54cc8ba981378399d2707 |
| 출처 메모 | uspto-grants-1999_03 |