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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1417421Generated: October 30, 2026

Hydrochloric Acid → 8-Amino-octanoic acid methyl-butyl-amide hydrochloric acid salt

https://huagongshe.com/reaction/1417421

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
Reactant8-(t-Butoxycarbonyl)amino-octanoic acid methyl-butyl-amideHCID 53721969—
Solvent1,4-DioxaneHCID 31275—
Product8-Amino-octanoic acid methyl-butyl-amide hydrochloric acid saltHCID 86753759—

Reaction Steps

Combine 8-(t-butoxycarbonyl)amino-octanoic acid methyl-butyl-amide and 4M hydrochloric acid in dioxane (10 mL). After 1 hour, the reaction mixture is evaporated in vacuo to give a residue. Triturate the residue with diethyl ether to give a solid. Collect the solid by filtration and dry in vacuo to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05877202
Source datasetuspto-grants-1999_03
ORD IDord-3745e05df16b4b459819b691d267c529
Source noteuspto-grants-1999_03