HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 8-Amino-octanoic acid methyl-butyl-amide hydrochloric acid salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 8-(t-Butoxycarbonyl)amino-octanoic acid methyl-butyl-amide | HCID 53721969 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 8-Amino-octanoic acid methyl-butyl-amide hydrochloric acid salt | HCID 86753759 | — |
Reaction Steps
Combine 8-(t-butoxycarbonyl)amino-octanoic acid methyl-butyl-amide and 4M hydrochloric acid in dioxane (10 mL). After 1 hour, the reaction mixture is evaporated in vacuo to give a residue. Triturate the residue with diethyl ether to give a solid. Collect the solid by filtration and dry in vacuo to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05877202 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-3745e05df16b4b459819b691d267c529 |
| Source note | uspto-grants-1999_03 |