HRID1417421

反应详情

EQUATION

反应方程式

HRID 1417421 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Combine 8-(t-butoxycarbonyl)amino-octanoic acid methyl-butyl-amide and 4M hydrochloric acid in dioxane (10 mL). After 1 hour, the reaction mixture is evaporated in vacuo to give a residue. Triturate the residue with diethyl ether to give a solid. Collect the solid by filtration and dry in vacuo to give the title compound.

WORKUP

后处理

  1. customthe reaction mixture is evaporated in vacuo
  2. customto give a residue
  3. customTriturate the residue with diethyl ether
  4. customto give a solid
  5. customCollect the solid
  6. filtrationby filtration
  7. customdry in vacuo