HRID1417421
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Combine 8-(t-butoxycarbonyl)amino-octanoic acid methyl-butyl-amide and 4M hydrochloric acid in dioxane (10 mL). After 1 hour, the reaction mixture is evaporated in vacuo to give a residue. Triturate the residue with diethyl ether to give a solid. Collect the solid by filtration and dry in vacuo to give the title compound.
WORKUP
后处理
- customthe reaction mixture is evaporated in vacuo
- customto give a residue
- customTriturate the residue with diethyl ether
- customto give a solid
- customCollect the solid
- filtrationby filtration
- customdry in vacuo