HCID 53957871, compound → HCID 53765476, compound

Participants

Reaction Steps

5 ml of formic acid was added to 51 mg of tert-butyl (1-methylthiocarbazol-2-yl)acetate, as obtained in Example 2. The reaction mixture was then warmed to room temperature and stirred for 4 hours. Formic acid was next removed under reduced pressure, and the residue was recrystallized from ethyl acetate and hexane, to yield 44 mg of the title compound, melting at 210°-212° C.

Provenance & Evidence