HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Benzyloxy)benzyl chloride → tert-Butyl [9-(3-Benzyloxybenzyl)-4-methyl-1-methylthiocarbazol-2-yl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Benzyloxy)benzyl chloride | HCID 13173490 | — |
| Reactant | Tert-butyl (4-methyl-1-methylthiocarbazol-2-yl)acetate | HCID 54527372 | — |
| Product | tert-Butyl [9-(3-Benzyloxybenzyl)-4-methyl-1-methylthiocarbazol-2-yl]acetate | HCID 57238596 | 78% |
Reaction Steps
Following a procedure and using relative proportions of starting materials similar to those described in Example 4, but using tert-butyl (4-methyl-1-methylthiocarbazol-2-yl)acetate and 3-benzyloxybenzyl chloride as starting materials, the title compound was obtained in a yield of 78% as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05877199 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-611981a98ec84ab692642e20de7ba35b |
| Source note | uspto-grants-1999_03 |