HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-(bromomethyl)-3-nitro- → tert-Butyl [4-Methyl-1-methylthio-9-(3-nitrobenzyl)carbazol-2-yl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-(bromomethyl)-3-nitro- | HCID 77568 | — |
| Reactant | Tert-butyl (4-methyl-1-methylthiocarbazol-2-yl)acetate | HCID 54527372 | — |
| Product | tert-Butyl [4-Methyl-1-methylthio-9-(3-nitrobenzyl)carbazol-2-yl]acetate | HCID 86753776 | 83% |
Reaction Steps
Following a procedure and using relative proportions of starting materials similar to those described in Example 4, but using tert-butyl (4-methyl-1-methylthiocarbazol-2-yl)acetate and 3-nitrobenzyl bromide as starting materials, the title compound was obtained in a yield of 83% as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05877199 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-0ec23b5e1adf4f4eac1038c7a94a7f5f |
| Source note | uspto-grants-1999_03 |