HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → tert-Butyl [9-Methylsulfonyl-4-methyl-1-methylthiocarbazol-2-yl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | Tert-butyl (4-methyl-1-methylthiocarbazol-2-yl)acetate | HCID 54527372 | — |
| Product | tert-Butyl [9-Methylsulfonyl-4-methyl-1-methylthiocarbazol-2-yl]acetate | HCID 54150576 | 95% |
Reaction Steps
Following a procedure and using relative proportions of starting materials similar to those described in Example 4, but using tert-butyl (4-methyl-1-methylthiocarbazol-2-yl)acetate and methylsulfonyl chloride as starting materials, the title compound was obtained in a yield of 95% as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05877199 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-723eaf619f754264903ca522aba4d768 |
| Source note | uspto-grants-1999_03 |