HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 70187550, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 70187500 | HCID 70187500 | — |
| Product | HCID 70187550 | HCID 70187550 | 81% |
Reaction Steps
Using an analogous procedure to that described in Example 25, 6-(3'-methylanilino)-4-[3'-(ethoxycarbonylmethoxy)anilino]pyrimidine was reacted with saturated methanolic ammonia to give 4-[3'-(carbamoylmethoxy)anilino]6-(3'-methylanilino)pyrimidine in 81% yield, m.p. 192°-194° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880130 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-f61122786bdc4d7681a5a08b8505a3c0 |
| Source note | uspto-grants-1999_03 |