HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 54117673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 53943104 | HCID 53943104 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54117673 | HCID 54117673 | 99% |
Reaction Steps
The method of Example 6 was repeated using methyl 4-cyclopropyl-4-(4-ethoxyphenyl)-2-fluorobut-2-enoate (Example 2) (1.2 g), diethyl ether (40 ml) and lithium aluminium hydride (0.2 g) to yield the title compound (1.05 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880162 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-d682d37897b9439da777ac8cd88ad4ab |
| Source note | uspto-grants-1999_03 |