HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 53811159, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 53652126 | HCID 53652126 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 53811159 | HCID 53811159 | 93% |
Reaction Steps
The method of Example 6 was repeated using methyl 2-fluoro-4-methyl-4-(4-trifluoromethoxyphenyl)pent-2-enoate (Example 5) (0.19 g), diethyl ether (10 ml) and lithium aluminium hydride (90 mg) to yield the title compound (0.16 g, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880162 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-db7bb7dac7a94541a8e5fbed271e0e0c |
| Source note | uspto-grants-1999_03 |