HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 53684786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 54117673 | HCID 54117673 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 53684786 | HCID 53684786 | 99% |
Reaction Steps
The method of Example 11 was repeated using acetyl chloride (1.2 ml), 4-cyclopropyl-4-(4-ethoxyphenyl)-2-fluorobut-2-enol (Example 7) (0.65 g), benzene (34 ml) and pyridine (0.24 ml) to yield the title compound (0.75 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880162 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-8deab34530924548939888fac036b0e8 |
| Source note | uspto-grants-1999_03 |