HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → 4-(4-Chlorophenyl)-2-fluoro-4-methylpent-2-enyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 4-(4-Chlorophenyl)-2-fluoro-4-methylpent-2-enol | HCID 53791045 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 4-(4-Chlorophenyl)-2-fluoro-4-methylpent-2-enyl acetate | HCID 53804842 | 87% |
Reaction Steps
The method of Example 11 was repeated using acetyl chloride (0.76 ml), 4-(4-chlorophenyl)-2-fluoro4-methylpent-2-enol (Example 8) (0.34 g), benzene (20 ml) and pyridine (0.15 ml) to yield the title compound (0.35 g, 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880162 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-895d64ec99ff4364ac623ed9bbae9390 |
| Source note | uspto-grants-1999_03 |