HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → 4-(4-Ethoxyphenyl)-2-fluoro-4-methylpent-2-enyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Acetate chloride | HCID 21917432 | — |
| Reactant | 4-(4-Ethoxyphenyl)-2-fluoro-4-methylpent-2-enol | HCID 53692153 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 4-(4-Ethoxyphenyl)-2-fluoro-4-methylpent-2-enyl acetate | HCID 54305003 | 99% |
Reaction Steps
The method of Example 11 was repeated using acetate chloride (0.17 ml), 4-(4-ethoxyphenyl)-2-fluoro-4-methylpent-2-enol (Example 9) (86 mg), benzene (4 ml) and pyridine (0.04 ml) to yield the title compound (0.1 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880162 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-6eabaceaecac46b6af189f4b22b0bdbc |
| Source note | uspto-grants-1999_03 |