HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 54398959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 53811159 | HCID 53811159 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 54398959 | HCID 54398959 | 99% |
Reaction Steps
The method of Example 11 was repeated using acetyl chloride (0.41 ml), 2-fluoro-4-methyl-4-(4-trifluoromethoxyphenyl)pent-2-enol (Example 10) (0.2 g), benzene (10 ml) and pyridine (0.081 ml) to yield the title compound (0.23 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880162 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-c7e55bdbd194499a8605f818f60b68d6 |
| Source note | uspto-grants-1999_03 |