HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 88136266, compound → Aminoacetaldehyde dimethyl acetal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 88136266 | HCID 88136266 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Aminoacetaldehyde dimethyl acetal | HCID 89728 | — |
| Product | HCID 88135642 | HCID 88135642 | — |
Reaction Steps
The N-[2-(1-benzyl-1-azoniabicyclo[2.2.2]-octan-4-yl)ethyl]aminoacetaldehyde-dimethylacetal-chloride-hydrochloride [melting point: 202°-204° C. (decomp.); Rf -value: 0.62 (Reversed Phase Silica gel, methanol/5% aqueous saline solution=6:4)]1 used as amine component is obtained by reaction of 1-benzyl-4-(2-chloroethyl)-1-azoniabicyclo[2.2.2]octane-chloride with aminoacetaldehyde-dimethylacetal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880284 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-e9ac3cdaf3b94380a4d3ae073c7482e0 |
| Source note | uspto-grants-1999_03 |