HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(2,4-Dimethoxy-5-formylphenyl)octanoic acid Methyl 3-(2,4-dimethoxy-5-formylphenyl)octanoate → Methyl 3-(2,4-dimethoxy-5-formylphenyl)octanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(2,4-Dimethoxy-5-formylphenyl)octanoic acid Methyl 3-(2,4-dimethoxy-5-formylphenyl)octanoate | HCID 86753868 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | Methyl 3-(2,4-dimethoxy-5-formylphenyl)octanoate | HCID 19348477 | — |
Reaction Steps
32(iii) 3-(2,4-Dimethoxy-5-formylphenyl)octanoic acid Methyl 3-(2,4-dimethoxy-5-formylphenyl)octanoate [prepared as described in step (ii) above] was hydrolyzed in a similar manner to that described in Preparation 7 to give the title compound as crystals, melting at 110°-111.5° C. (from ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880147 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-0d8526252f84461daa23f72dd13c4ca3 |
| Source note | uspto-grants-1999_03 |