HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-(2,4-dimethoxy-5-propionylphenyl)octanoate → 3-(2,4-Dimethoxy-5-propionylphenyl)octanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-(2,4-dimethoxy-5-propionylphenyl)octanoate | HCID 19348498 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | 3-(2,4-Dimethoxy-5-propionylphenyl)octanoic acid | HCID 19348556 | — |
Reaction Steps
The methyl 3-(2,4-dimethoxy-5-propionylphenyl)octanoate prepared as described in step (i) above was hydrolyzed in a similar manner to that described in Preparation 7 to give the title compound as crystals, melting at 92.5°-94° C. (from ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880147 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-458e3daa2a7c4ba28220265aa0ea7c70 |
| Source note | uspto-grants-1999_03 |