Hydrogen Peroxide → 5,5'-Dithiobis(1-methyltetrazole)

HRID 1418253Notes

Reaction equation

HRID 1418253 reaction equation
[SH:1][C:2]1[N:6]([CH3:7])[N:5]=[N:4][N:3]=1.O.OO>CO>[CH3:7][N:6]1[C:2]([S:1][S:1][C:2]2[N:6]([CH3:7])[N:5]=[N:4][N:3]=2)=[N:3][N:4]=[N:5]1

Participants

5

Reactant 3

HCID 784Hydrogen PeroxideHCID 962WaterHCID 178482017HCID 178482017, compound

Product 1

HCID 946035,5'-Dithiobis(1-methyltetrazole)

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Within a flask having a capacity of 1000 ml, 5-mercapto-1-methyltetrazole of 1000 mmol is solved in methanol of 450 ml, and the solution thus formed is cooled by water bathing. Into the solution thus prepared, 34.5% hydrogen peroxide of 20 ml is dropped slowly. At several minutes after dropping, the reaction generates heat, thus creating precipitate.

Workup

  1. customWithin a flask having
  2. customthe solution thus formed
  3. customInto the solution thus prepared
  4. waitAt several minutes after dropping
  5. temperaturethe reaction generates heat

Sources & evidence

ORD record
ord-a69624cf2d5a46cf8723ee23151f5701
Source dataset
uspto-grants-1999_03
Patent number
US05882819

Reaction notes

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