HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15428311, compound → HCID 15379550, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15428311 | HCID 15428311 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15379550 | HCID 15379550 | 71% |
Reaction Steps
In 20 ml of dichloromethane was suspended 0.211 g of 3-hydroxymethylimidazo[5,1-b]thiazole. Manganese dioxide (1.1 g) was added to the suspension, and the mixture was stirred at room temperature for 16 hr. The reaction mixture was filtered, and the filtrate was evaporated to dryness under reduced pressure to give 0.146 g (yield 71%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05883089 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-f3dfccc4e6984459b4bd698ccf4bae6f |
| Source note | uspto-grants-1999_03 |