HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Dimethylamino)phenol → HCID 67568574, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Dimethylamino)phenol | HCID 7421 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 67586931 | HCID 67586931 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67568574 | HCID 67568574 | — |
Reaction Steps
E-3-[3,5-Difluoro-4-(3-dimethylaminophenoxy)phenyl]-2-methyl-propenoic acid guanidide hydrochloride ##STR15## 10 a) The ester from 8 a, 3 eq. of potassium carbonate and 1.1 eq. of 3-dimethylaminophenol were stirred in DMF at 150° C. for 5 hours. After working up and purification, ethyl E-3-[3,5-difluoro-4-(3-dimethylaminophenoxy)phenyl]-2-methyl-propenoate was isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05883133 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-3537327bb628406280c0f8d83cd313a8 |
| Source note | uspto-grants-1999_03 |