HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Dimethylamino)phenol → HCID 67587604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Dimethylamino)phenol | HCID 7421 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 67568187 | HCID 67568187 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67587604 | HCID 67587604 | — |
Reaction Steps
11 b/12 b) The ester from 11 a/12 ma, 3 eq. of potassium carbonate and 1.1 eq. of 3-dimethylaminophenol were stirred in DMF at 150° C. for 3 hours. An isomer mixture of the ethyl esters of E-3-[2,6-difluoro-4-(3-dimethylaminophenoxy)]-2-methyl-propenoic acid and E-3-[2,4-difluoro-6-(3-dimethylaminophenoxy)-phenyl]-2-methyl-propenoic acid was isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05883133 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-7c3f6a4988cc47ff9775e91164541a0a |
| Source note | uspto-grants-1999_03 |