HRID1419474

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10942334

Methanol, sodium salt

CH3NaO

结构：CN(C)C=Nc1c(C(=O)CN)ncn1[C@@H]1O[C@H](CO)[C@@H](O)[C@H]1F

HCID53794522

未命名化合物

2 次

PRODUCTS

生成物

结构：O=C1CNC=Nc2c1ncn2[C@@H]1O[C@H](CO)[C@@H](O)[C@H]1F

HCID178516780

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

In step 18, compound (24) is dissolved in methanol and treated with a methanolic solution of sodium methylate at room temperature to effect the ring-formation of the substituents on the imidazole ring of compound (24). Thus, 3-(2-deoxy-2-fluoro-β-D-ribofuranosyl)-6,7-dihydroimidazo-[4,5-d] [1,3]diazepin-8(3H)-one [compound (25)] is produced.