HRID1419574

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID21863450

未命名化合物

结构：CN(c1ccccc1C1CCN(C(=O)OC(C)(C)C)CC1)S(C)(=O)=O

HCID67553893

未命名化合物

PRODUCTS

生成物

结构：CN(c1ccccc1C1CCNCC1)S(C)(=O)=O.O=C(O)C(F)(F)F

HCID86753991

未命名化合物

PROCEDURE

实验过程

N-[2-(1-t-Butoxycarbonylpiperidin-4-yl)phenyl]-N-methylmethanesulfonamide (662 mg) was dissolved in trifluoroacetic acid-dichloromethane (10%, 50 mL) and stirred at room temperature 2 h. The solvent was evaporated under reduced pressure to give the title compound as a colourless gum (670 mg), m/e (ES+) 269 (MH+).

WORKUP

后处理

customThe solvent was evaporated under reduced pressure