Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Phenylpyridine | HCID 13651 | — |
| Reactant | 1-Propanamine, 3-chloro-, hydrochloride | HCID 11469095 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67560974 | HCID 67560974 | 70.4% |
Reaction Steps
3-Chloropropylamine hydrochloride (13.0 g) and 15.5 g of 4-phenylpyridine were dissolved in dimethylacetamido and heated at 70° C. for 5 hours. Ethyl acetate was added thereto and the precipitated crystals were collected by filtration to obtain 17.5 g of 3-(4-phenylpyridyl)propylamine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05888694 |
|---|
| Source dataset | uspto-grants-1999_03 |
|---|
| ORD ID | ord-9654b29182c94a17a68863ef59db35a0 |
|---|
| Source note | uspto-grants-1999_03 |
|---|
