HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylbutanal → 1,3-Dioxane, 5-methyl-2-(2-methylpropyl)-, cis-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylbutanal | HCID 11552 | — |
| Reactant | Methylpropanediol | HCID 75103 | — |
| Product | 1,3-Dioxane, 5-methyl-2-(2-methylpropyl)-, cis- | HCID 23513560 | — |
Reaction Steps
2-isobutyl-5-methyl-1,3-dioxane was prepared on a laboratory scale by acid catalysed condensation of isovaleraldehyde and 2-methylpropane-1,3-diol using a 1 litre 3 necked flask equipped with a Dean and Stark condenser, a thermometer and a mechanical stirrer. The reaction scheme is shown in FIG. 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05888961 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-8cb8587b93e242d4aa5446d37300690c |
| Source note | uspto-grants-1999_03 |