HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butyl nitrite → HCID 351512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butyl nitrite | HCID 10906 | — |
| Reactant | Dimethyl Disulfide | HCID 12232 | — |
| Reactant | 2-Benzothiazolamine, dichloro- | HCID 112722 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 351512 | HCID 351512 | — |
Reaction Steps
43.7 g (0.47 mol) of dimethyl disulfide and 154.5 g (1.5 mol) of tert-butyl nitrite were added to a solution of 34 g (0.16 mol) of 2-amino-4,6-dichlorobenzothiazole in 1 liter of 1,2-dichloroethane. Stirring was carried out for 16 hours, followed by washing with water and 10% strength sodium hydroxide solution, drying over magnesium sulfate and evaporating down.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05888940 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-211d939a71ba483abfcada8ce673dd5f |
| Source note | uspto-grants-1999_03 |