HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1-Isothiocyanatoethyl)benzene → HCID 178462006, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1-Isothiocyanatoethyl)benzene | HCID 20559 | — |
| Reactant | 3-Amino-5-chlorothiophene-2-sulfonamide hydrochloride | HCID 68820626 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178462006 | HCID 178462006 | — |
Reaction Steps
The title compound was prepared from 3-amino-5-chlorothiophene-2-sulfonamide hydrochloride and L-α-methylbenzyl isothiocyanate by a procedure analogous to the procedure described in example 3Bc-d; mp 195°-204° C. (ethyl acetate), 1H-NMR (DMSO-d6): δ 1.46 (d, 3H), 4.95 (m, 1H), 7.1 (s, 1H), 7.2-7.45 (m, 5H), 7.78 (br. s, 1H), 10.85 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05889002 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-a3de523cf1a74128a15a36d6b42dcff4 |
| Source note | uspto-grants-1999_03 |