Benzyl Isothiocyanate → HCID 178527188, compound

HRID 1419750Notes

Reaction equation

HRID 1419750 reaction equation
Cl.[NH2:2][C:3]1[CH:7]=[C:6]([Cl:8])[S:5][C:4]=1[S:9]([NH2:12])(=[O:11])=[O:10].[CH2:13]([N:20]=[C:21]=S)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[CH2:13]([NH:20][C:21]1[NH:2][C:3]2[CH:7]=[C:6]([Cl:8])[S:5][C:4]=2[S:9](=[O:10])(=[O:11])[N:12]=1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

3

Reactant 2

HCID 2346Benzyl IsothiocyanateHCID 688206263-Amino-5-chlorothiophene-2-sulfonamide hydrochloride

Product 1

HCID 178527188HCID 178527188, compound

Procedure

The title compound was prepared from 3-amino-5-chlorothiophene-2-sulfonamide hydrochloride and benzyl isothiocyanate by a procedure analogous to the procedure described in example 3Bc-d; mp 223°-226° C.; 1H-NMR (DMSO-d6): δ 4.42 (d, 2H), 7.05 (s, 1H), 7.30 (m, 5H), 7.78 (br t, 1H), 11.22 (br s, 1H).

Sources & evidence

ORD record
ord-cfe527ee24b24ca2a2e845c5af2ecb3e
Source dataset
uspto-grants-1999_03
Patent number
US05889002

Reaction notes

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