1-Methylpiperazine → HCID 53723575, compound

HRID 1419769Notes

Reaction equation

HRID 1419769 reaction equation
[F:1][C:2]1[CH:3]=[C:4]2[C:16](=[O:17])[C:15]([C:18]([OH:20])=[O:19])=[CH:14][N:6]3[CH2:7][CH2:8][N:9]([CH3:13])[C:10]([C:11]=1F)=[C:5]23.[CH3:21][N:22]1[CH2:27][CH2:26][NH:25][CH2:24][CH2:23]1>>[F:1][C:2]1[CH:3]=[C:4]2[C:16](=[O:17])[C:15]([C:18]([OH:20])=[O:19])=[CH:14][N:6]3[CH2:7][CH2:8][N:9]([CH3:13])[C:10]([C:11]=1[N:25]1[CH2:26][CH2:27][N:22]([CH3:21])[CH2:23][CH2:24]1)=[C:5]23

Participants

3

Reactant 2

HCID 531671-MethylpiperazineHCID 69960914HCID 69960914, compound

Product 1

HCID 53723575HCID 53723575, compound

Procedure

Using 9,10-difluoro-1-methyl-7-oxo-2,3-dihydro-1H,7H-pyrido[1,2,3-de]quinoxaline-6-carboxylic acid and 4-methylpiperazine, the same procedure as in Production Example 1 was followed to yield the title compound.

Sources & evidence

ORD record
ord-764b322636014344b9989ed7b5fed7cd
Source dataset
uspto-grants-1999_03
Patent number
US05889009

Reaction notes

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