HRID1419795

反应详情

EQUATION

反应方程式

HRID 1419795 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

31.3 g (0.106 mol) of 4-(2-hydroxy-1,1,1-trifluoro-2-propyl)phenol benzyl ether were hydrogenated in 380 ml of glacial acetic acid in the presence of 6.3 g of palladium (5% on charcoal) at 50° C. After filtration to remove the catalyst and concentration, 18.9 g (87% of theory) remained of a colorless product.

WORKUP

后处理

  1. filtrationAfter filtration
  2. customto remove
  3. concentrationthe catalyst and concentration, 18.9 g (87% of theory)