HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178429769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 54040220 | HCID 54040220 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Rhodium | HCID 23948 | — |
| Product | HCID 178429769 | HCID 178429769 | — |
Reaction Steps
36 g (0.185 mol) of 4-(1-methylcyclohexyl)cyclohexanone were subjected to reductive amination in 210 ml of ammonia-saturated methanol in the presence of 3 g of rhodium (5% on charcoal) at 50° C. and 50 bar hydrogen pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05889012 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-1d4a242e7bd44363875f10758ad4e2ef |
| Source note | uspto-grants-1999_03 |