HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 69471538, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 16737206 | HCID 16737206 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 69471538 | HCID 69471538 | 54% |
Reaction Steps
Fluorothioacetamide (3.39 g) and benzyl bromide (6.23 g) were refluxed in chloroform (40 ml), under nitrogen, for 16 h. After cooling, the mixture was diluted with ether (200 ml) and the resulting orange solid filtered off. The solid was washed with more ether and dried over P2O5 in vacuo to give 5.19 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05889056 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-93a754e113f9425abbc9ad40dd8b8ff7 |
| Source note | uspto-grants-1999_03 |