HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 10562328, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Propylamine | HCID 7852 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 86754018 | HCID 86754018 | — |
| Product | HCID 10562328 | HCID 10562328 | 97% |
Reaction Steps
Following procedure A MeOH (0.8 mL) and propylamine (0.02 mL) were added to 2 (46.2 mg, 0.14 mmol) and stirred at room temperature for 2 days. Column chromatography with 3% ethyl acetate in petroleum ether gave pure yellow product in 97% yield (33.3 mg). Melting point 165°-167° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05889185 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-9a92e6eb7ca444ddb9e4e34a14f673ec |
| Source note | uspto-grants-1999_03 |