2-Methyl-1-butene → HCID 131721832, compound

Participants

Reaction Steps

100 ml of saturated β-cyclodextrin solution (1.8%) were cooled to 10° and mixed with 3 ml of 2-methyl-1-butene. The resulting difficultly soluble complex was precipitated with constant stirring in the ultrasonic bath. The deposit was obtained in crystalline form through freeze-drying and filtering. 2-methyl-1-butene content according to GC calculation: 0.82%

Provenance & Evidence