HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloropropane → HCID 131721833, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloropropane | HCID 6361 | — |
| Reactant | beta-Cyclodextrin | HCID 444041 | — |
| Product | HCID 131721833 | HCID 131721833 | — |
Reaction Steps
100 ml of saturated β-cyclodextrin solution (1.8%) were cooled to 10° C. and mixed with 3 ml of isopropylchloride. The resulting difficultly soluble complex was precipitated with constant stirring in the ultrasonic bath. The deposit was obtained in crystalline form through freeze-drying and filtering. Isopropylchloride content according to GC calculation: 0.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06071496 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-0878944c87504ce08b1125dba864f3fd |
| Source note | uspto-grants-2000_06 |