Methacrylic Acid → HCID 131721837, compound

HRID 1420485Notes

Reaction equation

HRID 1420485 reaction equation
[C:1]([O:6][C:7]12[CH2:16][CH:11]3[CH2:12][CH:13]([CH2:15][CH:9]([CH2:10]3)[CH2:8]1)[CH2:14]2)(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:17]([O:22][C:23]([CH3:26])([CH3:25])[CH3:24])(=[O:21])[C:18]([CH3:20])=[CH2:19].[C:27]([OH:32])(=[O:31])[C:28]([CH3:30])=[CH2:29]>O1CCCC1>[C:1]([O:6][C:7]12[CH2:16][CH:11]3[CH2:10][CH:9]([CH2:15][CH:13]([CH2:12]3)[CH2:14]1)[CH2:8]2)(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:17]([O:22][C:23]([CH3:26])([CH3:25])[CH3:24])(=[O:21])[C:18]([CH3:20])=[CH2:19].[C:27]([OH:32])(=[O:31])[C:28]([CH3:30])=[CH2:29]

Participants

5

Reactant 3

HCID 4093Methacrylic AcidHCID 11448tert-Butyl methacrylateHCID 109550921-Adamantyl methacrylate

Product 1

HCID 131721837HCID 131721837, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Adamantyl methacrylate (AMM), tert-butyl methacrylate (t-BM) and methacrylic acid (MA) were mixed together with tetrahydrofuran (THF) thereby to obtain a mixed solution, to which 10 mol. % of azoisobutyronitrile (AIBN) was added as an initiator. Then, the resultant mixture was allowed to undergo a reaction for 40 hours to obtain a copolymer (AMM-t-BM-MA; 35:40:25) having a molecular weight of 10,000.

Workup

  1. customto obtain a mixed solution
  2. customa reaction for 40 hours

Sources & evidence

ORD record
ord-75e9ee9df4324fccaa540a087f9d41b2
Source dataset
uspto-grants-2000_06
Patent number
US06071670

Reaction notes

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