HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 18781970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 18781937 | HCID 18781937 | — |
| Product | HCID 18781970 | HCID 18781970 | 80% |
Reaction Steps
Substituting 4-methylthio-1-phenacyl-azetidin-2-one (0.53 g, 2.25 mmol) for 4-methylthio-1-(9-phenyl-2-oxononyl)azetidin-2-one and using corresponding molar quantities of mCPBA as for Examples 5 and 6 gave 4-methylsulphinyl-1-phenacylazetidin-2-one (Example 8) as a waxy white solid (0.45 g, 80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06071899 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-802f8be5e1f440fcbd7713d260cec0e0 |
| Source note | uspto-grants-2000_06 |