HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 70299297, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 18782164 | HCID 18782164 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 70299297 | HCID 70299297 | — |
Reaction Steps
1-(3-Hydroxymethylphenyl)-5-methylbenzimidazole (0.3 g, 1.26 mM) was dissolved in dichloromethane (3 ml). Thionyl chloride (92 μl, 1.26 mM) was added and the reaction stirred for 30 minutes. Solvent evaporated to obtain product (0.36 g). MS M+ 957.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06071909 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-58ce5b30868d4b26a0ce586262eb4940 |
| Source note | uspto-grants-2000_06 |