Hydrochloric Acid → HCID 18782298, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 28.4 g (0.23 mol) of o-anisidine and 43.18 g (0.28 mol) of 1,1,1-trifluoro-2,4-pentanedione is heated at 100-105° C. for one hour and then cooled and the reaction medium is taken up with ethyl ether. 10 ml of 1 N hydrochloric acid are added. The mixture is filtered to remove the insoluble product, and the filtrate is concentrated under reduced pressure to give the expected product in the form of a beige solid (yield=98%).

Provenance & Evidence