HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178479544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Benzonitrile | HCID 7505 | — |
| Product | HCID 178479544 | HCID 178479544 | 96% |
Reaction Steps
A solution of benzonitrile (20 g, 0.194 mol) in methanol (8 ml) was bubbled with gaseous HCl to saturation. The solution was allowed to stand overnight, and then a pale yellow solid was found. The solid was triturated with ether, filtered, washed with ether, and dried to yield beige solid product (32 g, 96%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06071913 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-505d79f556dc4fb48946a5bf8ccee1ed |
| Source note | uspto-grants-2000_06 |