Hydrochloric Acid → HCID 178479544, compound

HRID 1420718Notes

Reaction equation

HRID 1420718 reaction equation
[C:1](#[N:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[ClH:9].C[OH:11]>>[ClH:9].[C:1](=[NH:8])([OH:11])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 7505Benzonitrile

Product 1

HCID 178479544HCID 178479544, compoundYield 96%

Procedure

A solution of benzonitrile (20 g, 0.194 mol) in methanol (8 ml) was bubbled with gaseous HCl to saturation. The solution was allowed to stand overnight, and then a pale yellow solid was found. The solid was triturated with ether, filtered, washed with ether, and dried to yield beige solid product (32 g, 96%).

Workup

  1. customThe solid was triturated with ether
  2. filtrationfiltered
  3. washwashed with ether
  4. customdried

Sources & evidence

ORD record
ord-505d79f556dc4fb48946a5bf8ccee1ed
Source dataset
uspto-grants-2000_06
Patent number
US06071913

Reaction notes

Loading…