HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminum(III) Chloride → HCID 9904289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 9948635 | HCID 9948635 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 9904289 | HCID 9904289 | — |
Reaction Steps
A solution of 0.6 mmol of the compound of Example 3 and an excess of aluminium chloride in chloroform is stirred at 50° C. for 30 minutes. After concentration under reduced pressure, the residue is stirred in water for 30 minutes to yield red crystals. After filtration, chromatography on silica gel (chloroform) allows the expected product to be isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06071945 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-e7ce1fff2fd24749add9ebd860db38d4 |
| Source note | uspto-grants-2000_06 |