HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 12128597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 12128596 | HCID 12128596 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12128597 | HCID 12128597 | — |
Reaction Steps
1mmol of the compound of Example 23 dissolved in an excess of hydrobromic acid in 33% acetic acid is stirred for 30 minutes at ambient temperature. After adding 100 ml of water, a precipitate is formed, which is filtered off and then dried. Chromatography on silica gel (ethyl acetate/hexane:1/2) allows the expected product to be isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06071945 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-772ea38848d24e82a1a0a3b17590c625 |
| Source note | uspto-grants-2000_06 |