HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl (3,3,5,5-tetramethylcyclohexylidene)acetate → HCID 18783146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl (3,3,5,5-tetramethylcyclohexylidene)acetate | HCID 15307456 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18783146 | HCID 18783146 | 95% |
Reaction Steps
Ethyl 3,3,5,5-tetramethylcyclohexylideneacetate (7) (4.48 g, 20 mmol) in ethanol (100 ml) was hydrogenated over 10% Pd/C (0.22 g, 5 wt. %) at 10 atm for 18 h. Filtration through Celite™ and evaporation afforded 4.28 g (95%) of 8 as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06071966 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-a9b2bd8216d747628cb396fe10c80f73 |
| Source note | uspto-grants-2000_06 |