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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1421142Generated: November 1, 2026

Ammonia → HCID 5327661, compound

https://huagongshe.com/reaction/1421142

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantHCID 14525670HCID 14525670—
SolventDimethylformamideHCID 6228—
ProductHCID 5327661HCID 5327661—

Reaction Conditions

Temperature130 °C

Reaction Steps

56 mg of 3-(1-methyl-3-indolyl)-4-(1-naphthyl)furan-2,5-dione were treated with 5 ml of DMF and 5 ml of 33% aqueous ammonia and the mixture was heated at 130° C. for 5 hours. The formed precipitate was filtered off, washed with water and dried to give 53 mg of 3-(1-methyl-3-indolyl)-4-(1-naphthyl)-1H-pyrrole-2,5-dione, m.p. 258°-260° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUSRE036736
Source datasetuspto-grants-2000_06
ORD IDord-a277174e14674a00947626d65525e760
Source noteuspto-grants-2000_06