HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-En-1-Ol → 3-Phenylprop-2-Enal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-En-1-Ol | HCID 308 | — |
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | Dodecane | HCID 8182 | — |
| Product | 3-Phenylprop-2-Enal | HCID 307 | — |
Reaction Steps
1.5 g (11.2 mmol) of cinnamyl alcohol (trans-3-phenyl-2-propen-1-ol), 36 g (367 mmol) of cyclohexanone, 0.5 g of catalyst and 1.5 g of dodecane (as GC standard) were heated under argon. After the end of the reaction time, the reaction mixture was analyzed by gas chromatography and the yield was determined. The results are summarized in Table 5 below:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06075145 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-86f9188a6a994c66af1b0d4e3b635a76 |
| Source note | uspto-grants-2000_06 |