HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenylethanol → Acetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenylethanol | HCID 7409 | — |
| Reactant | Cyclohexanone | HCID 7967 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Acetophenone | HCID 7410 | — |
Reaction Steps
5.0 g (40.9 mmol) of 1-phenylethanol, 15.0 g (153 mmol) of cyclohexanone and 1.0 g of catalyst from Example 9 in 30 g of toluene were heated at 70° C. under argon. After a reaction time of 10 hours, the reaction mixture was analyzed by gas chromatography. The yield of product was 94.2 percent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06075145 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-48f09b43e04d4a40b55c3d25141e90a7 |
| Source note | uspto-grants-2000_06 |